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  • Chem Sci Trans., 2017, 6(2),  pp 251-258  

    DOI:10.7598/cst2017.1370

    Research Article

    Studies on Heat Resistant Metal Composite of N-Substituted Maleimide

  • JYOTICHAUDHARY, SWATI PUROHIT* and SUMANJINGER
  • Department of Polymer Science, M.L. Sukhadia University, Udaipur -313001, (Rajasthan) India
  • Abstract

    N-(4-acetylphenyl)maleimide (APMI) was homopolymerized and copolymerized with acrylic acid (AA) at 60-70 oC in tetrahydrofuran (THF) solution with azoisobutyronitrile (AIBN) as an initiator. Metal composites were also synthesized with various metal such as, Fe+2, Co+2, Ni+2, Cu+2. The structure of monomer, homopolymer and copolymer, metal composites were elucidated by FT-IR, 1H-NMR and elemental analysis. The nine copolymer samples were synthesized from different feed ratio of comonomer. The monomer reactivity ratio rNAPMI and rAA were determined by Finemann Ross method. The investigated homo and copolymers showed solubility in polar solvents. Thermal behavior of homopolymer and copolymer were evaluated by TGA and DSC.The molecular weights were determined by GPC. The antimicrobial activity of synthesized homopolymer, copolymer and were screen against various bacteria and fungi and they showed excellent antimicrobial activity

    Keywords

    THF, Reactivity ratio, TGA, Finemann-ross method, Antimicrobial activity

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