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  • Chem Sci Trans., 2013, 2(3),  pp 829-834  

    DOI:10.7598/cst2013.438

    Research Article

    Crystal Growth and Characterization of 1-(2,4-Dichlorophenyl-2yl)-3-(4-hydroxyphenyl)prop-2-en-1-one

  • SHUBHALAXMI, STEPHANIE HAHNE, A. JAYARAMA and K. SUBRAHMANYA BHAT*
  • Department of Chemistry, Manipal Institute of Technology, Manipal University, Manipal-576104, India
    Technical University Munich, Wissenschaftszentrum Weihenstephan, Freising, Germany
    Department of Physics, Mangalore Institute of Technology & Engineering (MITE), Moodabidri-574 225, India
  • Abstract

    A potential crystal for nonlinear optical application and monomer namely 1-(2,4-dichloro-phenyl-2yl)-3-(4-hydroxyphenyl)prop-2-en-1-one (DHPP) was synthesized and grown by slow evaporation technique. The functional groups present in the compound were identified by FTIR spectrum. The optical cut-off wavelength and structural characteristics were analyzed using UV-Vis-NIR spectra and single crystal x-ray diffractometer. The crystal belongs to non centrosymmetric orthorhombic system with space group Pna21 with cell parameters a= 18.015(3) , b= 18.218(3), c= 4.1029(6) , Z=4 and V= 1346.563. Thermal studies show that the crystal is stable up to 250 0C implying good processability.

    Keywords

    Hydroxychalcone, Crystal growth, Single crystal studies, X-ray diffraction

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