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  • Chem Sci Trans., 2014, 3(2),  pp 642-645  

    DOI:10.7598/cst2014.767

    Research Article

    Microwave Assisted Oxidation of N,N-Dimethylaniline by Ditertiarybutyl Chromate in Non-Aqueous Media

  • RICHA KUMARI, SNIGDHA LAL, ANITA KUMARI GUPTA, SANGITA KATRE and HARI OM PANDEY
  • Departement of Chemistry, Ranchi University, Ranchi- 834008, Jharkhand, India
    Department of Chemistry, S S Memorial College, Ranchi University, Ranchi-834008, India
    Department of Chemistry, C J Patel Arts, Commerce, Science & Post-graduate College, Tirora, R T M Nagpur University, Maharashtra-441911, India
    Department of Chemistry, Ranchi University, Ranchi- 834008, Jharkhand, India
  • Abstract

    Microwave assisted organic synthesis has grown into a powerful tool in the hands of chemists. In the present paper we report the study of products of oxidation of N,N-dimethylaniline by ditertiary butyl chromate in few non aqueous solvents like acetonitrile, tetrahydrofuran and dioxane. The substrate solution and ditertiary butyl chromate was taken in appropriate ratio, mixed, stirred and irradiated in domestic microwave for the specified periods. The solid products of different colour and compositions so obtained were studied by elemental analysis, FTIR curves and thermogravimetric mass loss pattern.

    Keywords

    N,N-Dimethylaniline, Ditertiarybutylchromate, Dioxane, Tetrahydrofuran

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