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  • Chem Sci Trans., 2014, 3(4),  pp 1497-1501  

    DOI:10.7598/cst2014.903

    Research Article

    A Green Protocol for Synthesis of Some Novel 3-(2-Chloroquinolin-3-yl)acrylic Acid via Knoevenagal Reaction

  • R. A. SHASTRI* and P. P. JOSHI
  • Post Graduate Department of Chemistry, SBES College of Science, Aurangabad- 431001 (Maharashtra), India
  • Abstract

    A series of novel 3-(2-chloroquinolin -3- yl)acrylic acid derivatives (3a-j) were prepared by Knoevenagal condensation of 2-chloro 3-formyl quinoline (2a-j) with malonic acid (2) in the presence of catalytic quantity of pyridine under microwave irradiation in excellent yield with short time span (70 s). Newly synthesized compounds were characterized by IR, 1H NMR and mass.

    Keywords

    2-Chloro-3-formyl quinoline, Malonic acid, Pyridine, Acrylic acid, Microwave

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