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DMF Solvated Structure of 3'-[(4-Fluorophenyl)- carbonyl]-5'-[2-(methylsulfanyl)ethyl]-4'-(phenyl)spiro[indole-3,2'-pyrrolidin]-2(1H)-one:
A Pyrrolidine Alkaloidal Derivative
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DUBLIN | CORE | METADATA ITEM | METADATA FOR THIS DOCUMENT |
1 | Title | Title of Document | DMF Solvated Structure of 3'-[(4-Fluorophenyl)- carbonyl]-5'-[2-(methylsulfanyl)ethyl]-4'-(phenyl)spiro[indole-3,2'-pyrrolidin]-2(1H)-one:
A Pyrrolidine Alkaloidal Derivative
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2 | Creator | Author's name, affiliation, country | PREETIKA SHARMA1, M. SAPNAKUMARI2, B. NARAYANA2,
B.K.SAROJINI3 and RAJNI KANT1*
1X-ray Crystallography Laboratory, Department of Physics, University of Jammu,
Jammu-Tawi-180006, India
2Department of Studies in Chemistry, Mangalore University,
Mangalagangotri-574199, India
3 Department of Industrial Chemistry, Mangalore University, Mangalagangotri-574199, India
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3 | Subject | Dicipline(s) | Chemical Science |
3 | Subject | Keywords | Spiro-oxindole, Pyrrolidine, Direct method, Crystal structure, Intermolecular interactions |
4 | Description | Abstract | The compound 3'-[(4-fluorophenyl)carbonyl]-5'-[2-(methylsulfanyl)ethyl]4'-(phenyl) spiro[indole-3,2'-pyrrolidin]-2(1H)-one, C30H31FN3O3S, crystallizes in the orthorhombic space group P212121 with unit cell parameters, a = 6.3529(8) Å, b = 11.4335(14) Å, c = 38.405(4) Å, α = β = γ = 90.0o, Z=4. The crystal structure was solved by direct methods. The data were collected at room temperature (293 K) and the structure was refined by full-matrix least-squares procedures to a final R-value of 0.1015 for 3630 observed reflections. The molecular structure is stabilized by one intra [C-H?O] and one DMF-guided inter [N-H?O] molecular interaction. Besides this, few CH∙∙∙π interactions have also been observed |
5 | Publishers | Organizing agency, location | WWW Publications, India |
6 | Contributor | Sponsor(s) | - |
7 | Date | Date (YYYY-MM-DD) | - |
8 | Type | Status & genre | Peer-reviewed Article |
8 | Type | Type | |
9 | Formate | File Formate | PDF |
10 | Identifier | Uniform Resource Identifier | Click Here |
10 | Identifier | Digital Object Identifier | |
11 | Source | Journal/conference title; vol., no. (Year) | Chemical Science Transactions, Volume 4 , Number (4), (2015) |
12 | Lanuguage | English=en | en |
13 | Relation | Supp.files | |
14 | Coverage | | - |
15 | Copyright | Copyright and permissions | |
Chemical Science Transactions | Chem Sci Trans | CST | Online Chemistry Journal | Open Access
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