| DUBLIN | CORE | METADATA ITEM | METADATA FOR THIS DOCUMENT |
| 1 | Title | Title of Document | Convenient Preparation of Mono-2 or Mono-3-O-Benzoyl-ß-Cyclodextrin Dependent the Solvent Equilibrium |
| 2 | Creator | Author's name, affiliation, country | ZHI-ZHONG WANG
Engineering Research Center for Hui Medicine Modernization, School of Pharmacy, Ningxia Medical University, Yinchuan, Ningxia, 750004, P. R. China |
| 3 | Subject | Dicipline(s) | Chemical Science |
| 3 | Subject | Keywords | Cyclodextrin, Benzoylation, Isomerization, Equilibrium |
| 4 | Description | Abstract | A new and convenient method is presented for the preparation of mono-2 or mono-3-O-benzoyl-ß-cyclodextrin by direct benzoylation of ß-cyclodextrin on the secondary hydroxyl face using N-benzoylimidazole in carbonate buffer solution. These processes involved the solvent-dependent equilibriums of isomerization to improve the yields. Among the common solvents
(N,N-dimethylform-amide, dimethyl sulfoxide and H2O), dimethyl sulfoxide is the most advantageous for preparing mono-2-O-benzoyl-ß-cyclodextrin and H2O is the most advantageous for preparing mono-3-O-benzoyl-ß-cyclodextrin. |
| 5 | Publishers | Organizing agency, location | WWW Publications, India |
| 6 | Contributor | Sponsor(s) | - |
| 7 | Date | Date (YYYY-MM-DD) | - |
| 8 | Type | Status & genre | Peer-reviewed Article |
| 8 | Type | Type | |
| 9 | Formate | File Formate | PDF |
| 10 | Identifier | Uniform Resource Identifier | Click Here |
| 10 | Identifier | Digital Object Identifier | |
| 11 | Source | Journal/conference title; vol., no. (Year) | Chemical Science Transactions, Volume 1 , Number (1), (2012) |
| 12 | Lanuguage | English=en | en |
| 13 | Relation | Supp.files | |
| 14 | Coverage | | - |
| 15 | Copyright | Copyright and permissions | |
