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Synthesis, Spectral Characterization and Biological Screening of Potentially Active 1, 3-Diones and its Transition Metal Complexes |
DUBLIN | CORE | METADATA ITEM | METADATA FOR THIS DOCUMENT |
1 | Title | Title of Document | Synthesis, Spectral Characterization and Biological Screening of Potentially Active 1, 3-Diones and its Transition Metal Complexes |
2 | Creator | Author's name, affiliation, country | D. M. SURYAWANSHI, V. D. INGLE, N. A. BHISE, A. S. RAJBHOJ and S. T. GAIKWAD* Department of Chemistry, Rayat Shikshan Sanstha?s Annasaheb Awate College,
Manchar (M.S.), 410 503, India
Department of Chemistry, Dr. Babasaheb Ambedkar Marathwada University,
Aurangabad (M.S.), 431 004, India
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3 | Subject | Dicipline(s) | Chemical Science |
3 | Subject | Keywords | 1, 3-Diones, Metal complexes, Ultrasound irradiations, Magnetic measurements, Antibacterial screening |
4 | Description | Abstract | 1-(2-Hydroxyphenyl)-3-propane-1, 3-diones 4(LA-LB) and its metal complexes 5(a-e) have been newly synthesized from substituted 2-hydroxyacetophenones 1(A-B) and aromatic acids 2(A-B) under ultrasound irradiation method at low temperature. These compounds were characterized by FT-IR, UV-Vis., 1H-NMR, 13C-NMR, mass spectroscopy and magnetic measurement. The stoichiometry of the complexes was found 1:2 (metal:ligand). The physicochemical data suggested octahedral geometry for all the complexes. The ligands 4(LA-LB) and their metal complexes 5(a-e) were screened for in vitro antibacterial activity against S. aureus, B. subtilis, E. coli and P. aeruginosa compared with tetracycline and chloramphenicol as a standard drugs. The results are in good agreement with respect to activity of free ligand and its metal complexes. Reactions under ultrasonic irradiation had improved yield. |
5 | Publishers | Organizing agency, location | WWW Publications, India |
6 | Contributor | Sponsor(s) | - |
7 | Date | Date (YYYY-MM-DD) | - |
8 | Type | Status & genre | Peer-reviewed Article |
8 | Type | Type | |
9 | Formate | File Formate | PDF |
10 | Identifier | Uniform Resource Identifier | Click Here |
10 | Identifier | Digital Object Identifier | |
11 | Source | Journal/conference title; vol., no. (Year) | Chemical Science Transactions, Volume 5 , Number (4), (2016) |
12 | Lanuguage | English=en | en |
13 | Relation | Supp.files | |
14 | Coverage | | - |
15 | Copyright | Copyright and permissions | |
Chemical Science Transactions | Chem Sci Trans | CST | Online Chemistry Journal | Open Access
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