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Synthesis and Crystal Structure of 2-[(4-Chlorobenzoyl)amino]-3-(4-formylphenyl)prop-2-enoic Acid |
| DUBLIN | CORE | METADATA ITEM | METADATA FOR THIS DOCUMENT |
| 1 | Title | Title of Document | Synthesis and Crystal Structure of 2-[(4-Chlorobenzoyl)amino]-3-(4-formylphenyl)prop-2-enoic Acid |
| 2 | Creator | Author's name, affiliation, country | SANJAY KUMAR, K. N. SUBBULAKSHMI, B. NARAYANA, B. K. SAROJINI, SUMATI ANTHAL and RAJNI KANT*
X-ray Crystallography Laboratory, Department of Physics,
University of Jammu, Jammu-Tawi-180006, India
Department of Chemistry, Mangalore University,
Mangalagangothri-574199, D.K., Mangalore, India
Department of Industrial Chemistry, Mangalore University,
Mangalagangothri- 574 199, D.K., Mangalore, India
Department of Chemistry, Shree MadhwaVadiraja Institute of Technology and Management (VTU Belgaum), Vishwothama Nagar, Bantakal, Udupi-574115, Karnataka, India
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| 3 | Subject | Dicipline(s) | Chemical Science |
| 3 | Subject | Keywords | Chlorobenzoyl, Benzaldehyde, Direct methods, Hydrogen bonds, Dimer |
| 4 | Description | Abstract | 2-[(4-Chlorobenzoyl)amino]-3-(4-formylphenyl)prop-2-enoic acid (C17H12ClNO4) crystallizes in the orthorhombic space group Pbcn with unit cell parameters: a = 17.2460(13) Å, b = 9.6735(8) Å, c = 19.953(2) ?, α = β= γ = 90.00 o and Z=8. Direct methods were used to solve the crystal structure and refined by full matrix least squares proc?dures to final R value of 0.0675 for 1294 observed reflections. The crystal structure is stabilized by N?H⋅⋅⋅O, O?H⋅⋅⋅O and C?H⋅⋅⋅O hydrogen bonds. The dimer molecule is linked through a bifurcated(acceptor) hydrogen bond (N1-H1?O4,C17-H17?O4). |
| 5 | Publishers | Organizing agency, location | WWW Publications, India |
| 6 | Contributor | Sponsor(s) | - |
| 7 | Date | Date (YYYY-MM-DD) | - |
| 8 | Type | Status & genre | Peer-reviewed Article |
| 8 | Type | Type | |
| 9 | Formate | File Formate | PDF |
| 10 | Identifier | Uniform Resource Identifier | Click Here |
| 10 | Identifier | Digital Object Identifier | |
| 11 | Source | Journal/conference title; vol., no. (Year) | Chemical Science Transactions, Volume 6 , Number (1), (2017) |
| 12 | Lanuguage | English=en | en |
| 13 | Relation | Supp.files | |
| 14 | Coverage | | - |
| 15 | Copyright | Copyright and permissions | |
Chemical Science Transactions | Chem Sci Trans | CST | Online Chemistry Journal | Open Access
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