Chemical Science Transactions | Chem Sci Trans | CST | Online Chemistry Journal | Open Access
Home | Table of Contents | Submit an article | Subscribe | Login | Register

Indexing Metadata

Synthesis of Some Polyamides from Bis(thiosemicarbazone)acenaphthenequinone

DUBLINCOREMETADATA ITEM METADATA FOR THIS DOCUMENT
1TitleTitle of DocumentSynthesis of Some Polyamides from Bis(thiosemicarbazone)acenaphthenequinone
2CreatorAuthor's name, affiliation, country NAVABEH NAMI, HOSSEIN MIGHANI, NAJMEH KIA and HAMED SADATFARAJI
Department of Chemistry, Qaemshahr Branch, Islamic Azad University, Qaemshahr, Mazandaran Iran
Department of Chemistry, University of Golestan, Gorgan, Iran
3SubjectDicipline(s) Chemical Science
3SubjectKeywords Polyamides, Thermalstability, Bisthiosemicarbazone, Acenaphthoquinone, Diacide
4DescriptionAbstract Bis(thiosemicarbazone)acenaphthenequinon (LH6) was synthesized in one step from acenaphthoquinone and thiosemicarbazone. The diamine (LH6) was characterized by FT-IR, 1H NMR and melting point. diamine was used to prepare novel polyamides. The low temperature solution polycondensation of ligand with aromatic ring. Diacid chlorides and high temperature polycondensation with dicarboxylic acid afforded ligand-containing polyamides with inherent viscosities of 0.31–0.38 dL/g in N-methylpyrolidone at 25 oC. The polyamides were generally soluble in a wide range of solvents such as dimethyformamide(DMF), N-Methylpyrolidone(NMP), dimthylsulfoxide (DMSO) and H2SO4. Thermal analysis showed that these polyamides were practically amorphous and exhibited 10% weight loss at and above 220 oC.
5PublishersOrganizing agency, location WWW Publications, India
6Contributor Sponsor(s) -
7DateDate (YYYY-MM-DD) -
8TypeStatus & genre Peer-reviewed Article
8TypeType
9FormateFile Formate PDF
10IdentifierUniform Resource Identifier Click Here
10IdentifierDigital Object Identifier
11SourceJournal/conference title; vol., no. (Year)Chemical Science Transactions, Volume  2 , Number  (S1), (2013)
12LanuguageEnglish=en en
13RelationSupp.files
14Coverage -
15CopyrightCopyright and permissions
Chemical Science Transactions | Chem Sci Trans | CST | Online Chemistry Journal | Open Access
Home | Table of Contents | Submit an article | Subscribe | Login | Register