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Microwave Assisted Synthesis, Characterization and Antimicrobial Study of Substituted Benzo-(5,6-e)-[1,3]-diazepine-4,7-dione Derivatives |
DUBLIN | CORE | METADATA ITEM | METADATA FOR THIS DOCUMENT |
1 | Title | Title of Document | Microwave Assisted Synthesis, Characterization and Antimicrobial Study of Substituted Benzo-(5,6-e)-[1,3]-diazepine-4,7-dione Derivatives |
2 | Creator | Author's name, affiliation, country | RAJESH M. KHARATE, PRADIP P. DEOHATE and B. N. BERAD Department of Chemistry, Shri Sant Gajanan Maharaj College of Engineering, Shegaon, Dist.-Buldhana, India
Department of Chemistry, Shri Radhakisan Laxminarayan Toshniwal College of Science, Akola, India
Department of Chemistry, Rashtrasant Tukadoji Maharaj Nagpur University, Nagpur, India |
3 | Subject | Dicipline(s) | Chemical Science |
3 | Subject | Keywords | Benzodiazepine-di-ones, Microwave assisted synthesis, Antimicrobial activity |
4 | Description | Abstract | Synthesis of series of [benzo-(5,6-e)-1,3-diphenyl-2-arylimino-[1,3]-diazepine]-4,7-dione hydrochlorides have been achieved by the interaction of N,N-diphenyl phthalamide with N-aryl isocyanodichlorides by irradiation in a domestic microwave oven for specified time using little chloroform as a solvent along with potassium carbonate. The hydrochlorides were then basified with dilute ammonium hydroxide solution. The parent compound N,N-diphenyl phthalamide was obtained by refluxing the mixture of phthalic anhydride and aniline in toluene. The structures of synthesized compounds were established on the basis of chemical transformation, elemental analysis, IR, 1H NMR and Mass spectral studies. The synthesized compounds have been assayed for their antimicrobial activity against gram-positive as well as gram-negative microorganisms. |
5 | Publishers | Organizing agency, location | WWW Publications, India |
6 | Contributor | Sponsor(s) | - |
7 | Date | Date (YYYY-MM-DD) | - |
8 | Type | Status & genre | Peer-reviewed Article |
8 | Type | Type | |
9 | Formate | File Formate | PDF |
10 | Identifier | Uniform Resource Identifier | Click Here |
10 | Identifier | Digital Object Identifier | |
11 | Source | Journal/conference title; vol., no. (Year) | Chemical Science Transactions, Volume 2 , Number (1), (2013) |
12 | Lanuguage | English=en | en |
13 | Relation | Supp.files | |
14 | Coverage | | - |
15 | Copyright | Copyright and permissions | |
Chemical Science Transactions | Chem Sci Trans | CST | Online Chemistry Journal | Open Access
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