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Microwave Assisted Synthesis, Characterization and Antimicrobial Study of Substituted Benzo-(5,6-e)-[1,3]-diazepine-4,7-dione Derivatives

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1TitleTitle of DocumentMicrowave Assisted Synthesis, Characterization and Antimicrobial Study of Substituted Benzo-(5,6-e)-[1,3]-diazepine-4,7-dione Derivatives
2CreatorAuthor's name, affiliation, country RAJESH M. KHARATE, PRADIP P. DEOHATE and B. N. BERAD
Department of Chemistry, Shri Sant Gajanan Maharaj College of Engineering, Shegaon,
Dist.-Buldhana, India
Department of Chemistry, Shri Radhakisan Laxminarayan Toshniwal College of Science,
Akola, India
Department of Chemistry, Rashtrasant Tukadoji Maharaj Nagpur University, Nagpur, India
3SubjectDicipline(s) Chemical Science
3SubjectKeywords Benzodiazepine-di-ones, Microwave assisted synthesis, Antimicrobial activity
4DescriptionAbstract Synthesis of series of [benzo-(5,6-e)-1,3-diphenyl-2-arylimino-[1,3]-diazepine]-4,7-dione hydrochlorides have been achieved by the interaction of N,N-diphenyl phthalamide with N-aryl isocyanodichlorides by irradiation in a domestic microwave oven for specified time using little chloroform as a solvent along with potassium carbonate. The hydrochlorides were then basified with dilute ammonium hydroxide solution. The parent compound N,N-diphenyl phthalamide was obtained by refluxing the mixture of phthalic anhydride and aniline in toluene. The structures of synthesized compounds were established on the basis of chemical transformation, elemental analysis, IR, 1H NMR and Mass spectral studies. The synthesized compounds have been assayed for their antimicrobial activity against gram-positive as well as gram-negative microorganisms.
5PublishersOrganizing agency, location WWW Publications, India
6Contributor Sponsor(s) -
7DateDate (YYYY-MM-DD) -
8TypeStatus & genre Peer-reviewed Article
8TypeType
9FormateFile Formate PDF
10IdentifierUniform Resource Identifier Click Here
10IdentifierDigital Object Identifier DOI:10.7598/cst2013.287
11SourceJournal/conference title; vol., no. (Year)Chemical Science Transactions, Volume  2 , Number  (1), (2013)
12LanuguageEnglish=en en
13RelationSupp.files
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Chemical Science Transactions | Chem Sci Trans | CST | Online Chemistry Journal | Open Access
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