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Synthesis, Characterization and Thermogravimetric Analysis of 2,2-Biphenol Based Terpolymer Resins

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1TitleTitle of DocumentSynthesis, Characterization and Thermogravimetric Analysis of 2,2-Biphenol Based Terpolymer Resins
2CreatorAuthor's name, affiliation, country PRIYANKA U. BELSARE and ANIL B. ZADE
Professor of Chemistry, Department of Chemistry, Laxminarayan Institute of Technology, Rashtrasant Tukdoji Maharaj, Nagpur University, Nagpur-440 010, India
3SubjectDicipline(s) Chemical Science
3SubjectKeywords Synthesis, Characterization, Thermogravimetry, Kinetic parameters
4DescriptionAbstract The novel terpolymer resins (2,2-BPTEPAF- I, II, III) have been synthesized by condensation polymerization of 2,2-biphenol (2,2-BP) and tetraethylenepentamine (TEPA) with formaldehyde (F) in presence of 2 M NaOH as a catalyst using varying molar ratios of reacting monomers. The composition of resins has been determined by elemental analysis. Spectral studies such as UV-Visible, FT-IR and 1H NMR spectra have been used to confine the most probable structures of newly synthesized terpolymer resins. Non-isothermal thermogravimetric analysis has been carried out to determine their mode of decomposition and relative thermal stability. Kinetic parameters such as energy of activation (Ea), order of reaction (n) and frequency factor (z) has been calculated by applying Friedman, Chang and Sharp-Wentworth methods. The computed results are compared and elaborated.
5PublishersOrganizing agency, location WWW Publications, India
6Contributor Sponsor(s) -
7DateDate (YYYY-MM-DD) -
8TypeStatus & genre Peer-reviewed Article
8TypeType
9FormateFile Formate PDF
10IdentifierUniform Resource Identifier Click Here
10IdentifierDigital Object Identifier DOI:10.7598/cst2013.488
11SourceJournal/conference title; vol., no. (Year)Chemical Science Transactions, Volume  2 , Number  (4), (2013)
12LanuguageEnglish=en en
13RelationSupp.files
14Coverage -
15CopyrightCopyright and permissions
Chemical Science Transactions | Chem Sci Trans | CST | Online Chemistry Journal | Open Access
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