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Synthesis, Characterisation and Thermal Behaviour of Salicylates of Heterobimetallic [Ca(II)-Sn(IV)]-μ-Oxoisopropoxide

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1TitleTitle of DocumentSynthesis, Characterisation and Thermal Behaviour of Salicylates of Heterobimetallic [Ca(II)-Sn(IV)]-μ-Oxoisopropoxide
2CreatorAuthor's name, affiliation, country RAJESH KUMAR and RAJVINDER KAUR
Department of Chemistry, HCTM Technical Campus, Kaithal -136027, India
Department of Chemistry, Singhania University, Pacheri Bari, Jhunjhunu -333515, Rajasthan, India
3SubjectDicipline(s) Chemical Science
3SubjectKeywords Heterobimetallic--oxoisopropoxide, Calcium, Tin, Salicylates, Thermal analysis
4DescriptionAbstract The heterobimetallic-μ-oxoisopropoxide [CaO2Sn2(OPri)6] provides different salicylate derivatives of the type [CaO2(Sn2((OPri)6-n(RSAL)n] (where n is 1-4 and RSAL = Salicylate anion) with methyl salicylate (HRSAL1), ethyl salicylate (HRSAL2) and phenyl salicylate (HRSAL3). The derivatives have been characterized by elemental, spectral (IR, 1H, 13C NMR), thermal and molecular weight measurement. The hydrolyzed product of these salicylate derivatives obtained by hydrothermally assisted sol-gel process favors the formation of multicomponent oxides subject to their thermal study. The studies reveal that salicylate derivatives are monomeric in nature and low susceptible to hydrolysis in comparison to parent compound and may prove excellent precursors for the mixed metal oxides.
5PublishersOrganizing agency, location WWW Publications, India
6Contributor Sponsor(s) -
7DateDate (YYYY-MM-DD) -
8TypeStatus & genre Peer-reviewed Article
8TypeType
9FormateFile Formate PDF
10IdentifierUniform Resource Identifier Click Here
10IdentifierDigital Object Identifier DOI:10.7598/cst2014.659
11SourceJournal/conference title; vol., no. (Year)Chemical Science Transactions, Volume  3 , Number  (1), (2014)
12LanuguageEnglish=en en
13RelationSupp.files
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