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UV Assay Method for the Determination of Doxycycline Hyclate in Bulk and Pharmaceutical Formulation

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1TitleTitle of DocumentUV Assay Method for the Determination of Doxycycline Hyclate in Bulk and Pharmaceutical Formulation
2CreatorAuthor's name, affiliation, country V. SREERAM*, A. V. D. NAGENDRAKUMAR1, SRINIVASA RAO KARUMURI2 and M. MADHU3
*P.G. Department of Chemistry, A.G & S.G. Siddhartha College of Arts & Science, Vuyyuru-521 165, India
iDepartment of Chemistry, GITAM University, Visakhapatnam-530 045, Andhra Pradesh, India
2Department of Electronics & Instrumentation, Lakireddy Bali Reddy College of Engineering, Mylavaram, A.P, India
3Department of Chemistry, P.B. Siddhartha College of Arts & Science, Vijayawada, A.P. India
3SubjectDicipline(s) Chemical Science
3SubjectKeywords Doxycycline hyclate, RP-HPLC, UV detection, Recovery
4DescriptionAbstract A simple, selective, linear, precise and accurate UV Assay method was developed and validated for rapid assay of Doxycycline hyclate in bulk and pharmaceutical formulation. For this development paddle apparatus were used. The purified water was used as dissolution medium and solvent. Stirring rate was employed at 75 rpm and the withdrawal time was identified as 30 minutes and the filter size was found to be 0.45 μ m at ambient temperature. The method was validated as per the ICH guidelines. The method was successfully applied for routine analysis of Doxycycline hyclate in the rapid and reliable determination in pharmaceutical formulation.
5PublishersOrganizing agency, location WWW Publications, India
6Contributor Sponsor(s) -
7DateDate (YYYY-MM-DD) -
8TypeStatus & genre Peer-reviewed Article
8TypeType
9FormateFile Formate PDF
10IdentifierUniform Resource Identifier Click Here
10IdentifierDigital Object Identifier DOI:10.7598/cst2015.909
11SourceJournal/conference title; vol., no. (Year)Chemical Science Transactions, Volume  4 , Number  (1), (2015)
12LanuguageEnglish=en en
13RelationSupp.files
14Coverage -
15CopyrightCopyright and permissions
Chemical Science Transactions | Chem Sci Trans | CST | Online Chemistry Journal | Open Access
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